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DTIC ADA1003533: A Study of Mechanical Alloying of Metal Powders
by Defense Technical Information Center
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This investigation was undertaken primarily to obtain
information concerning the chemical and structural
homogeneity of mechanically alloyed powders and to
determine under what conditions, if any, true solid
solutions may be formed. Four different alloy systems
were selected for study: (1) 50 w/o Cr - 50 w/o Mo, (2)
Type 316 stainless steel, (3) 20.8 w/o Mn - 79.2 w/o Bi,
and (4) a Beta-Ti alloy (Ti-11Cr-8Mn-5Mo-3Al). In both
the Cr-Mo system and Type 316 stainless steel system, it
was established by x-ray diffraction methods that the
elemental components had become interdispersed on an
atomic scale as a result of high-energy milling, but that
a minimum threshold speed is necessary to obtain a
significant degree of alloying. However, annealing
studies on the milled powders provided strong indications
that the solid solutions formed by mechanical alloying
are very inhomogeneous from a chemical and structural
point of view. Milling difficulties were encountered with
the Beta-Ti and Bi-Mn powder systems which precluded any
conclusions pertaining to structural or chemical
homogeneity in these systems. In both the Bi-Mn and Beta-
Ti systems, the tendency toward cold-welding and/or
diffusion bonding of the particles was so pronounced that
it was not possible to achieve a proper balance of cold-
welding and particle fracturing in order to mechanically
alloy component metals.
Date Published: 2020-01-24 04:44:06
Identifier: DTIC_ADA1003533
Item Size: 59340151
Language: english
Media Type: texts
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DTIC Archive; Wassel, T K ; ARMY TAN...
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